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本文介紹了采用配置 APCI 源的 Agilent 6470 三重四極桿液質(zhì)聯(lián)用系統(tǒng)，同時檢測沙坦藥物中六種亞硝胺類基因毒性雜質(zhì) NDMA、NDEA、NMBA、NEIPA、NDIPA 和 NDBA 的方法。
本文介紹了采用 Agilent Ultivo 三重四極桿液質(zhì)聯(lián)用系統(tǒng)檢測氯沙坦鉀中的亞硝胺類雜質(zhì) NMBA 的方法。該方法采用常規(guī) ESI 源，即可獲得滿足檢測要求的分析結(jié)果，且方法簡單、特異性高、靈敏度高，大大優(yōu)于 FDA 官網(wǎng)公布的限量要求。