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The detection of low-level impurities contained in a sample of a structurally related main compound using high?resolution sampling 2D-LC is shown.
利用基于閥切換的2D-LC技術(shù)實(shí)現(xiàn)在不改變?cè)忌V條件的情況下，將某些質(zhì)譜不兼容的流動(dòng)相替換為質(zhì)譜兼容的流動(dòng)相，從而實(shí)現(xiàn)蛋白類樣品中雜質(zhì)的質(zhì)譜定性分析。